2-Chloro-N,N-dimethylacetamide

  • Name: 2-Chloro-N,N-dimethylacetamide
  • CAS: 2675-89-0
  • Purity: 99%
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1.What is the 2-Chloro-N,N-dimethylacetamide ?

2-Chloro-N,N-dimethylacetamide (N,N-dimethylchloroacetamide) was used in the synthesis of (S)-carbinoxamine.

dimethyl amine
124-40-3

dimethyl amine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N,N-dimethylacetamide
2675-89-0

2-chloro-N,N-dimethylacetamide

Conditions
Conditions Yield
With sodium hydrogencarbonate; In toluene; at -2 - 5 ℃; for 1h; Reagent/catalyst; Solvent; Temperature;
93.1%
With triethylamine; In dichloromethane; at -5 - 20 ℃; for 13h; Inert atmosphere;
93.09%
In diethyl ether; at 20 ℃; Cooling;
81%
With sodium hydroxide; In dichloromethane; for 0.25h;
79%
With sodium hydroxide; In water; 1,2-dichloro-ethane; at -15 ℃; for 0.75h;
66%
With potassium carbonate; In tetrahydrofuran; dichloromethane; at -20 ℃; for 1h;
48%
With alkali;
With sodium hydroxide; ammonia; In 1,2-dichloro-ethane; at -15 - -10 ℃; for 0.75h;
In benzene; for 1h; Reflux;
In benzene; at 10 ℃; for 1.5h; Reflux;
In dichloromethane; at -10 - 5 ℃; for 1h; pH=4 - 7;
In dichloromethane; water; at 5 - 10 ℃; for 1.33h; pH=4 - 7;
31 g
With sodium acetate; In dichloromethane; at 0 ℃;
With potassium carbonate; In acetonitrile; at 20 ℃; for 4h;
dimethyl amine; With triethylamine; In chloroform; at 0 ℃; Cooling with ice;
chloroacetyl chloride; In chloroform; at 0 - 20 ℃; for 4h;
With triethylamine; at 0 - 20 ℃; for 4h;
With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 1h; Cooling with ice;
With triethylamine; In dichloromethane; at 0 ℃; for 6h; Inert atmosphere;
In dichloromethane; at 10 - 15 ℃; for 2h;
N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N,N-dimethylacetamide
2675-89-0

2-chloro-N,N-dimethylacetamide

Conditions
Conditions Yield
With triethylamine; In dichloromethane; at 15 ℃;
77%
With triethylamine; In dichloromethane; at 0 ℃; for 3h;
62%
With sodium hydroxide; In 1,2-dichloro-ethane; at -5 ℃; for 0.5h;
33%
With sodium hydroxide; In diethyl ether; at -10 ℃; for 2h;
18%
With triethylamine; In dichloromethane; at 20 ℃; for 6h;
With triethylamine; In dichloromethane; at 0 ℃; for 4h;

2.What is the CAS number for 2-Chloro-N,N-dimethylacetamide ?

The CAS number of 2-Chloro-N,N-dimethylacetamide is 2675-89-0.

More information of 2-Chloro-N,N-dimethylacetamide 2675-89-0 are:

CAS?Number

2675-89-0

Density

1.101 g/cm3

Melting Point

-20 C

Boiling Point

173.2 °C at 760 mmHg

Flash Point

58.5 °C

Vapor Pressure

1.28mmHg at 25°C

Refractive Index

n20/D 1.479

HS CODE

H2CON(CH3)2 MOL WT. 121.57

PSA

20.31000

LogP

0.31340

Pka

-0.95±0.70(Predicted)

3.What are another words for 2-Chloro-N,N-dimethylacetamide ?

Synonyms?for?2-Chloro-N,N-dimethylacetamide 2675-89-0:2-Chloro-N,N'-dimethylacetamide;2-Chlorodimethylacetamide;N,N-Dimethyl-2-chloroacetamide;N,N-Dimethyl-a-chloroacetamide;N,N-Dimethylchloroacetamide;NSC1193;a-Chloro-N,N-dimethylacetamide;

4.What is the molecular formula of 2-Chloro-N,N-dimethylacetamide?

The chemical formula of ?2-Chloro-N,N-dimethylacetamide is?C4H8ClNO which containing 4 Carbon atoms,8 Hydrogen atoms,1 Chlorine atoms,1 Nitrogen atoms and 1 Oxygen atoms,and the molecular weight of??2-Chloro-N,N-dimethylacetamide?is 121.567.

5.What is 2-Chloro-N,N-dimethylacetamide (2675-89-0) used for?

2-Chloro-N,N-dimethylacetamide, also known as N,N-dimethylchloroacetamide, is an N,M-dialkyl amide that serves as an organic catalyst in various chemical reactions. It is characterized by the presence of a chloro group attached to the carbonyl carbon, with two methyl groups attached to the nitrogen atom. This unique structure endows it with properties that make it a valuable component in the synthesis of various compounds.

InChI:InChI=1/C4H8ClNO/c1-6(2)4(7)3-5/h3H2,1-2H3

Relevant articles related to 2-Chloro-N,N-dimethylacetamide:

Article

Source

-

Gurka,Taft

, p. 4794,4797, 4798 (1969)

Palladium-Catalyzed β-C(sp3)-H Arylation of Aliphatic Ketones Enabled by a Transient Directing Group

Wang, Yangyang,Wu, Gaorong,Xu, Xiaobo,Pang, Binghan,Liao, Shaowen,Ji, Yafei

, p. 7296 - 7303 (2021/05/29)

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