Details
Reliable Quality 2-Butylbenzofuran 4265-27-4 Hot Sale with Chinese Manufacturer
- Molecular Formula:C12H14O
- Molecular Weight:174.243
- Appearance/Colour:pale yellow
- Vapor Pressure:0.039mmHg at 25°C
- Refractive Index:1.5330
- Boiling Point:248.1 °C at 760 mmHg
- Flash Point:101.1 °C
- PSA：13.14000
- Density:1.011 g/cm3
- LogP:3.77540
2-Butylbenzofuran(Cas 4265-27-4) Usage
InChI:InChI=1/C12H14O/c1-2-3-7-11-9-10-6-4-5-8-12(10)13-11/h4-6,8-9H,2-3,7H2,1H3
4265-27-4 Relevant articles
Acid-promoted selective synthesis of trifluoromethylselenolated benzofurans with Se-(trifluoromethyl) 4-methylbenzenesulfonoselenoate
Liu, Juyan,Tian, Miaomiao,Li, Ankun,Ji, Liangshuo,Qiu, Di,Zhao, Xia
supporting information, (2021/02/01)
A Br?nsted acid-promoted trifluoromethyl...
Palladium complexes with an annellated mesoionic carbene (MIC) ligand: Catalytic sequential Sonogashira coupling/cyclization reaction for one-pot synthesis of benzofuran, indole, isocoumarin and isoquinolone derivatives
Bera, Jitendra K.,Daw, Prosenjit,Reshi, Noor U Din,Tyagi, Akshi
supporting information, p. 15238 - 15248 (2020/11/18)
Two Pd(ii) complexes (1 and 2) featuring...
PALLADIUM ACYCLIC DIAMINOCARBENE COMPLEXES AS PRECATALYSTS FOR HIYAMA COUPLING AND THE TANDEM ONE-POT FLUORIDE FREE HIYAMA COUPLING/CYCLIZATION FOR THE SYNTHESIS OF BIOLOGICALLY RELEVANT
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Paragraph 0108; 0109; 0114-0115, (2020/05/06)
The present invention provides Acyclic d...
A 2 - substituted benzofuran compound of the catalytic synthesis method
-
Paragraph 0016; 0017; 0018, (2019/05/22)
The invention discloses a 2 - substitute...
4265-27-4 Process route
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125345-27-9
2-(hex-1-yn-1-yl)phenol
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![2-n-butylbenzo[b]furan](/upload/2026/10/d9c0dd2e26a74054bdcce2040db639da_95da7859-f20d-4972-b196-13fe44eb29da.png)
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4265-27-4
2-n-butylbenzo[b]furan
| Conditions | Yield |
|---|---|
|
2-(hex-1-yn-1-yl)phenol;
With
N,N,N,N,-tetramethylethylenediamine; diethylzinc;
In
toluene;
at 120 ℃;
for 1h;
With
ammonium chloride;
In
toluene;
|
99% |
|
2-(hex-1-yn-1-yl)phenol;
With
n-butyllithium;
In
diethyl ether; hexane;
at 0 - 20 ℃;
for 30h;
With
zinc(II) chloride;
In
toluene;
at 120 ℃;
for 1h;
With
ammonium chloride;
In
water; toluene;
|
98% |
|
With
caesium carbonate; copper(l) chloride;
In
acetonitrile;
at 20 ℃;
for 6h;
under 760.051 Torr;
|
91.8% |
|
With
acetylacetonatodicarbonylrhodium(l); 1,1'-bisnaphthalene;
In
water; toluene;
at 100 ℃;
for 1h;
Inert atmosphere;
|
88% |
|
With
(acetylacetonato)dicarbonylrhodium (l); water; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
toluene;
at 100 ℃;
for 1h;
|
88% |
|
With
indium (III) iodide;
In
1,2-dichloro-ethane;
at 80 ℃;
regioselective reaction;
Schlenk technique;
Inert atmosphere;
|
86% |
|
With
cesium hydroxide;
In
1-methyl-pyrrolidin-2-one;
at 70 ℃;
for 2h;
|
65% |
|
With
potassium carbonate;
In
water;
at 110 ℃;
for 2h;
Microwave irradiation;
Inert atmosphere;
Green chemistry;
|
29% |
-
-
533-58-4
2-Iodophenol
-
-
693-02-7
hex-1-yne
-
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4265-27-4
2-n-butylbenzo[b]furan
| Conditions | Yield |
|---|---|
|
With
copper(l) iodide; tetra-(n-butyl)ammonium iodide; potassium carbonate; palladium;
In
toluene;
at 40 ℃;
Reagent/catalyst;
Temperature;
Inert atmosphere;
|
96.6% |
|
With
potassium carbonate;
at 60 ℃;
for 1h;
|
91% |
|
With
copper(l) iodide; L-proline; sodium hydroxide;
In
dimethyl sulfoxide;
at 80 ℃;
for 12h;
Inert atmosphere;
Sealed tube;
|
85% |
|
With
copper(l) iodide; potassium tert-butylate; trans-1,2-cyclohexanediamine;
In
1,4-dioxane;
at 125 ℃;
Inert atmosphere;
Sealed tube;
|
79% |
|
With
Pd-Cu/C; ethanolamine; triphenylphosphine;
In
water;
at 80 ℃;
for 20h;
Sealed tube;
Inert atmosphere;
|
73% |
|
With
copper(l) iodide; potassium hydroxide;
In
1,4-dioxane;
at 100 ℃;
for 108h;
Inert atmosphere;
|
48% |
|
With
potassium phosphate; diethylzinc; N,N`-dimethylethylenediamine;
In
acetonitrile;
at 125 ℃;
for 12h;
Sealed tube;
Inert atmosphere;
|
40% |
|
With
caesium carbonate; lithium chloride;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 15h;
|
35% |
|
Multi-step reaction with 2 steps
1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / Inert atmosphere
2: indium (III) iodide / 1,2-dichloro-ethane / 80 °C / Schlenk technique; Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; indium (III) iodide; triethylamine;
In
tetrahydrofuran; 1,2-dichloro-ethane;
|
|
|
With
C53H43IN3P2Pd(1+)*I(1-); potassium carbonate;
In
dimethyl sulfoxide;
at 90 ℃;
for 2h;
|
97 %Chromat. |
4265-27-4 Upstream products
-
271-89-6
1-benzofurane
-
542-69-8
1-iodo-butane
-
139-02-6
sodium phenoxide
-
70339-99-0
(2-Pentanoyloxy-benzyl)-triphenyl-phosphonium; bromide
4265-27-4 Downstream products
-
199725-34-3
1-[3-(2-butylbenzofuranyl)]-2-phenylethanone
-
94968-16-8
1-<3-(2-butylbenofuranyl)>-2-(4-methoxyphenyl)ethanone
-
796072-17-8
(4-bromo-phenyl)-(2-butyl-benzofuran-3-yl)-methanone
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83790-87-8
2-n-butyl 3-(4-methoxy benzoyl)-benzofuran
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